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Performance and mechanism for cadmium and lead adsorption from water and soil by corn straw biochar

Tong Chi,Jiane Zuo,Fenglin Liu

《环境科学与工程前沿（英文）》 2017年 第11卷 第2期 doi: 10.1007/s11783-017-0921-y

摘要： Corn straw biochar prepared under 400 °C was the best Cd and Pb adsorption capacity Maximum adsorption capacity of Cd and Pb were 43.48 and 22.73 mg·g , respectively The dominant mechanism of Cd and Pb adsorption was precipitation Biochar could reduce the bioavailability of heavy metals when mixed with soil Cadmium (Cd) and lead (Pb) in water and soil could be adsorbed by biochar produced from corn straw. Biochar pyrolyzed under 400°C for 2 h could reach the ideal removal efficiencies (99.24% and 98.62% for Cd and Pb, respectively) from water with the biochar dosage of 20 g·L and initial concentration of 20 mg·L . The pH value of 4–7 was the optimal range for adsorption reaction. The adsorption mechanism was discussed on the basis of a range of characterizations, including X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), Fourier transform infrared spectroscopy (FTIR) and Raman analysis; it was concluded as surface complexation with active sorption sites (-OH, -COO-), coordination with π electrons (C= C, C= O) and precipitation with inorganic anions (OH , CO , SO ) for both Cd and Pb. The sorption isotherms fit Langmuir model rather than Freundlich model, and the saturated sorption capacities for Cd and Pb were 38.91 mg·g and 28.99 mg·g , respectively. When mixed with soil, biochar could effectively increase alkalinity and reduce bioavailability of heavy metals. Thus, biochar derived from corn straw would be a green material for both removal of heavy metals and amelioration of soil.

关键词： Corn straw     Biochar     Heavy metals     Sorption isotherm     Bioavailability    

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METAGENOMICS COMBINED WITH HIGH-THROUGHPUT SEQUENCING REVEALS THE METHANOGENIC POTENTIAL OF FRESH CORNSTRAW UNDER THERMOPHILIC AND HIGH OLR

《农业科学与工程前沿（英文）》 2023年 第10卷 第3期   页码 403-423 doi: 10.15302/J-FASE-2022471

摘要：

● Methane production from fresh straw was 7.50% higher than dry straw.

关键词： fresh corn straw     high solid anaerobic digestion     metagenomics     microbial communities     thermophilic    

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Removing phosphorus from aqueous solutions by using iron-modified corn straw biochar

Fenglin LIU,Jiane ZUO,Tong CHI,Pei WANG,Bo YANG

《环境科学与工程前沿（英文）》 2015年 第9卷 第6期   页码 1066-1075 doi: 10.1007/s11783-015-0769-y

摘要： Iron-modified corn straw biochar was used as an adsorbent to remove phosphorus from agricultural runoff. When agricultural runoffs with a total phosphorus (TP) concentration of 1.86 mg·L to 2.47 mg·L were filtered at a hydraulic retention time of 2 h through a filtration column packed with the modified biochar, a TP removal efficiency of over 99% and an effluent TP concentration of less than 0.02 mg·L were achieved. The isotherms of the phosphorus adsorption by the modified biochar fitted the Freundlich equation better than the Langmuir equation. The mechanism of the phosphorus adsorbed by the modified biochar was analyzed by using various technologies, i.e. scanning electron microscopy (SEM), X-ray diffraction (XRD) analysis, X-ray photoelectron spectroscopy (XPS), and Fourier transform infrared spectroscopy (FTIR). The results indicated that the surface of the modified biochar was covered by small iron granules, which were identified as Fe O . The results also showed that new iron oxides were formed on the surface of the modified biochar after the adsorption of phosphorus. Moreover, new bonds of Fe-O-P and P-C were found, which suggested that the new iron oxides tend to be Fe (PO ) (OH) . Aside from removing phosphorus, adding the modified biochar into soil also improved soil productivity. When the modified biochar-to-soil rate was 5%, the stem, root, and bean of broad bean plants demonstrated increased growth rates of 91%, 64%, and 165%, respectively.

关键词： iron-modified biochar     phosphorus removal     agricultural waste     agricultural runoff    

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Experimental study on influence of operating parameters on tar components from corn straw gasification

Shuai GUO, Xiao WEI, Deyong CHE, Hongpeng LIU, Baizhong SUN

《能源前沿（英文）》 2021年 第15卷 第2期   页码 374-383 doi: 10.1007/s11708-020-0710-3

摘要： Gasification is a promising approach for converting solid fuel sources, including renewable ones like biomass, for use. The main problem in biomass gasification is the formation of condensable tars, including polycyclic aromatic hydrocarbons (PAHs). This paper investigated the conversion of tar components during corn straw gasification. It analyzed collected tar components using a gas chromatograph-mass spectrograph (GC-MS). Experimental results indicate that, with increasing temperature from 700°C to 900°C, the concentrations of benzene, indene, phenanthrene, naphthalene, acenaphthylene, fluorene, and pyrene increased whereas those of toluene, phenol, 1-methylnaphthalene, and 2-methylnaphthalene decreased. As the equivalence ratio (ER) increased from 0.21 to 0.34, the concentrations of indene and phenanthrene increased from 0.148% and 0.087% to 0.232% and 0.223%, respectively. Further, the phenol content increased as ER increased from 0.21 to 0.26 and then decreased as the ER increased further to 0.34. Other parameters like the steam/biomass (S/B) ratio and catalyst also played a critical role in tar reduction. This paper demonstrates the conversion of some tar components and elucidates their chemical properties during gasification.

关键词： gasification     tar components     operating parameters    

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Kinetic studies of xylan hydrolysis of corn stover in a dilute acid cycle spray flow-through reactor

Hongman ZHANG, Qiang JIN, Rui XU, Lishi YAN, Zengxiang LIN

《化学科学与工程前沿（英文）》 2011年 第5卷 第2期   页码 252-257 doi: 10.1007/s11705-010-1010-y

摘要： Xylan of corn stover was pretreated with 1%, 2% and 3% (w/w) sulfuric acid at relatively low temperatures (90°C, 95°C and 100°C) in a dilute acid cycle spray flow-through reactor (DCF). The hydrolysis of xylan to its monomeric xylose was modeled by a series of first-order reactions. Both biphasic and Saeman hydrolysis models were applied to fit the experimental data. The results confirmed that the kinetic data of xylan hydrolysis fitted a first-order irreversible reaction model and the experimental data. The reaction rates of xylose monomer formation and degradation were sensitive to catalyst concentration and temperature. Higher catalyst concentration and lower reaction temperature result in high xylose yield. The activation energy for xylose formation and degradation were determined to be 112.9 and 101.0 kJ·mol , respectively. Over 90% theoretical xylose obtained from corn stover can be used to produce ethanol, xylitol and fumaric acid by fermentation.

关键词： corn stover     xylan hydrolysis     biphasic model     Saeman model     cycle spray     kinetics    

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A neural network-based production process modeling and variable importance analysis approach in corn

《化学科学与工程前沿（英文）》 2023年 第17卷 第3期   页码 358-371 doi: 10.1007/s11705-022-2190-y

摘要： Corn to sugar process has long faced the risks of high energy consumption and thin profits. However, it’s hard to upgrade or optimize the process based on mechanism unit operation models due to the high complexity of the related processes. Big data technology provides a promising solution as its ability to turn huge amounts of data into insights for operational decisions. In this paper, a neural network-based production process modeling and variable importance analysis approach is proposed for corn to sugar processes, which contains data preprocessing, dimensionality reduction, multilayer perceptron/convolutional neural network/recurrent neural network based modeling and extended weights connection method. In the established model, dextrose equivalent value is selected as the output, and 654 sites from the DCS system are selected as the inputs. LASSO analysis is first applied to reduce the data dimension to 155, then the inputs are dimensionalized to 50 by means of genetic algorithm optimization. Ultimately, variable importance analysis is carried out by the extended weight connection method, and 20 of the most important sites are selected for each neural network. The results indicate that the multilayer perceptron and recurrent neural network models have a relative error of less than 0.1%, which have a better prediction result than other models, and the 20 most important sites selected have better explicable performance. The major contributions derived from this work are of significant aid in process simulation model with high accuracy and process optimization based on the selected most important sites to maintain high quality and stable production for corn to sugar processes.

关键词： big data     corn to sugar factory     neural network     variable importance analysis    

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Direct ethanol production from rice straw by coculture with two high-performing fungi

Maki TAKANO, Kazuhiro HOSHINO

《化学科学与工程前沿（英文）》 2012年 第6卷 第2期   页码 139-145 doi: 10.1007/s11705-012-1281-6

摘要： To develop efficient and economical direct ethanol production from fine rice straw crashed mechanically, two high-performing fungi, which can secret hyperactive cellulases and/or ferment effectively various sugars, were selected from some strains belong to preserved in our laboratory. The simultaneous saccharification and fermentation (SSF) by coculture with these fungi was investigated. The screening of high-performing fungi resulted in the selection of NBRC 4572 as an ethanol-producing fungus and NBRC 5398 as a cellulase-secreting fungus. The strain 4572 produced ethanol aerobically from glucose and xylose in high yields of 0.420 g/g at 36 h and 0.478 g/g at 60 h, respectively, but secreted fairly low cellulases. On the other hand, the strain 5398 also produced ethanol from glucose in yield of 0.340 g/g though it had a little growth in xylose culture. However, it secreted hyperactive cellulases that are essential for hydrolysis of rice straw in culture and the maximum activities of endo-β-glucanase and β-glucosidase were 2.11 U/L and 1.47 U/L, respectively. In SSF of rice straw by coculture with two fungi selected, the ethanol production reached 1.28 g/L after 96 h when the inoculation ratio of the strain 5398 to the strain 4572 was 9.

关键词： Mucor circinelloides     ethanol production     cellulase secretion     SSF     coculture     rice straw    

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Fabrication of cellulose aerogel from wheat straw with strong absorptive capacity

Jian LI,Caichao WAN,Yun LU,Qingfeng SUN

《农业科学与工程前沿（英文）》 2014年 第1卷 第1期   页码 46-52 doi: 10.15302/J-FASE-2014004

摘要： An effectively mild solvent solution containing NaOH/PEG was employed to dissolve the cellulose extracted from the wheat straw. With further combined regeneration process and freeze-drying, the cellulose aerogel was successfully obtained. Scanning electron microscope, X-ray diffraction technique, Fourier transform infrared spectroscopy, and Brunauer-Emmett-Teller were used to characterize this cellulose aerogel of low density (about 40 mg·cm ) and three-dimensional network with large specific surface area (about 101 m ·g ). Additionally, with a hydrophobic modification by trimethylchlorosilane, the cellulose aerogel showed a strong absorptive capacity for oil and dye solutions.

关键词： cellulose aerogel     absorptive capacity     waste wheat straw     freeze-drying    

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Isolation of highly purity cellulose from wheat straw using a modified aqueous biphasic system

Lifeng YAN, Yi ZHAO, Qing GU, Wan LI

《化学科学与工程前沿（英文）》 2012年 第6卷 第3期   页码 282-291 doi: 10.1007/s11705-012-0901-5

摘要： Cellulose samples with molecular weights ranging from 8.39 × 10 to 11.00 × 10 g/mol were obtained from wheat straw. The dewaxed wheat straw was pretreated with aqueous hydrochloric acid followed by delignification using an environmentally benign poly(ethyleneglycol)/salt aqueous biphasic system. The yield of cellulose was in the range of 48.9%–55.5% and the cellulose contained 1.2%–3.2% hemicelluloses, and 0.97%–3.47% lignin. All the isolated cellulose samples could be directly dissolved in a 6 wt-% NaOH/4 wt-% urea aqueous solution through a precooling-thawing process to form a homogenous solution. The separation process was investigated and the obtained cellulose and its solution were characterized by Fourier transform infrared spectroscopy, scanning electron microscopy and energy dispersive X-ray apparatus, and X-ray diffraction. The results revealed that aqueous soluble cellulose can be directly prepared from wheat straw by this method and this study opens a novel pathway to prepare cellulosic materials from agricultural waste.

关键词： cellulose     straw     separation     aqueous solution    

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Integrated benefits of power generation by straw biomass —A case study on the Sheyang Straw Power Plants

Xiaoshun LI , Futian QU , Dongmei JIANG , Peixin ZHU ,

《环境科学与工程前沿（英文）》 2009年 第3卷 第3期   页码 348-353 doi: 10.1007/s11783-009-0026-3

摘要： Power generation using straw biomass has quantifiable benefits from an economic, ecological, and sociological perspective in China. The methods used to construct the assessment models of these integrated benefits were the revenue capitalization approach and the discounted-cash-flow approach. The results indicated that a straw power plant with the capacity of 2.50×10 W and burning 1.23×10 tons of cotton straw could annually supply 1.40×10 kWh of power. However, it would not be until six years later that these results could be measured. Over the long term, the gross benefits could reach up to 4.63×10 Yuan. Therefore, the total benefits are expected to be 1.18 × 10 Yuan if all available straw resources are used to generate power. The policy implication showed that the long-term integrated benefits of power generation by straw biomass outweighed the short-term benefits. This is the main incentive to use straw biomass for power generation in the future.

关键词： straw biomass resources     power generation     renewable energy     Sheyang county    

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Detoxification and concentration of corn stover hydrolysate and its fermentation for ethanol production

Qing Li, Yingjie Qin, Yunfei Liu, Jianjun Liu, Qing Liu, Pingli Li, Liqiang Liu

《化学科学与工程前沿（英文）》 2019年 第13卷 第1期   页码 140-151 doi: 10.1007/s11705-018-1714-y

摘要： Environmental and energy concerns have increased interest in renewable energy sources, particularly biofuels. Thus the fermentation of glucose from sulfuric acid-hydrolyzed corn stover for the production of bioethanol has been explored using a combined acid retardation and continuous-effect membrane distillation treatment process. This process resulted in the separation of the sugars and acids from the acid-catalyzed hydrolysate, the removal of most of the fermentation inhibitors from the hydrolysate and the concentration of the detoxified hydrolysate. The recovery rate of glucose from the sugar-acid mixture using acid retardation was greater than 99.12% and the sulfuric acid was completely recovered from the hydrolysate. When the treated corn stover hydrolysate, containing 100 g/L glucose, was used as a carbon source, 43.06 g/L of ethanol was produced with a productivity of 1.79 g/(L?h) and a yield of 86.31%. In the control experiment, where glucose was used as the carbon source these values were 1.97 g/(L?h) and 93.10% respectively. Thus the integration of acid retardation and a continuous-effect membrane distillation process are effective for the production of fuel ethanol from corn stover.

关键词： corn stover     hydrolysate     acid retardation     continuous-effect membrane distillation     ethanol fermentation    

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Biological pretreatment of corn stover by solid state fermentation of

Jian ZHANG, Xin REN, Wenqun CHEN, Jie BAO

《化学科学与工程前沿（英文）》 2012年 第6卷 第2期   页码 146-151 doi: 10.1007/s11705-012-1220-6

摘要： Biological pretreatment is a promising way to overcome the biorecalcitrance of cleaving the supermolecular structure of lignocellulose by lignin degrading enzymes from microorganisms. Solid state fermentation of corn stover with the white-rot fungus was carried out and the efficiency of this pretreatment was evaluated. The enzymatic hydrolysis yield reached a maximum when the corn stover was biologically pretreated for nine days, and the hydrolysis yield decreased sharply if the solid state fermentation was carried out for more than nine days. A possible explanation for this sharp decrease is that not only the lignin degrading enzymes (LiP and MnP) were secreted, but also other metabolites, which were toxic or fatal to the hydrolysis enzymes resulting in the lower hydrolysis yield were generated during the prolonged period of biopretreatment. These results are useful to help determine the optimal timing and to understand the lignin structure and degradation mechanism in biological pretreatment processes.

关键词： biological pretreatment     Phanerochaete chrysosporium     solid state fermentation     biorecalcitrance     hydrolysis yield    

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Effect of mulching with maize straw on water infiltration and soil loss at different initial soil moistures

Yifu ZHANG,Hongwen LI,Jin HE,Qingjie WANG,Ying CHEN,Wanzhi CHEN,Shaochun MA

《农业科学与工程前沿（英文）》 2016年 第3卷 第2期   页码 161-170 doi: 10.15302/J-FASE-2016104

摘要： Mulching and soil water content (SWC) have a significant impact on soil erosion, and this study investigated the effect of straw mulching on water infiltration and soil loss under different initial SWC treatments in a rainfall simulation experiment conducted in northern China. Increasing initial SWC can decrease soil infiltration and increase soil loss. During an 80 mm rainfall event (80 mm·h for 60 min), 8%, 12% and 16% initial SWC treatments decreased cumulative infiltration by 8.7%, 42.5% and 58.1%, and increased total sediment yield by 44, 146 and 315 g, respectively, compared to 4% initial SWC. However, in all the straw mulching treatments, there was no significant difference in stable infiltration rate between the different initial SWC treatments. For all initial SWC treatments, straw mulching of 30% or more significantly enhanced water infiltration by over 31% and reduced soil loss by over 49%, compared to the unmulched treatment. Taking into consideration the performance of no-till planters, a maize straw mulching rate of 30% to 60% (1400–3100 kg·hm ) is recommended for the conservation of water and soil in northern China.

关键词： infiltration     initial soil water content     rainfall simulation     soil loss     straw mulching    

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Effects of cotton straw amendment on soil fertility and microbial communities

Wuren HUANG, Zhihui BAI, Daniel HOEFEL, Qing HU, Xin LV, Guoqiang ZHUANG, Shengjun XU, Hongyan QI, Hongxun ZHANG

《环境科学与工程前沿（英文）》 2012年 第6卷 第3期   页码 336-349 doi: 10.1007/s11783-011-0337-z

摘要： Maintaining soil fertility, while controlling pollution from excessive chemical fertilizer application is important for keeping soil productivity of sustainable agriculture. Variety of straws have been used and proven to be good soil amendments for increasing soil organic matter (OM) and a range of additional soil nutrients. However, little is known about the utilization of cotton straw for soil amendment. To better understand the mechanism behind cotton straw soil amendments, investigations were performed upon cucumber seedlings, where changes to soil nutrients and microbial communities were investigated. The results revealed that the cotton straw application promoted the cucumber seedling growth by significantly increasing the soil OM, available nitrogen, available phosphorus, and available potassium. The concentration of cotton straw was positively correlated to both the number of the culturable microorganisms and also the total microbial biomass within soil. Furthermore, assessment of cotton straw application using Biolog metabolic profiling and phospholipid fatty acid analysis revealed that such application increased the microbial community metabolic activity, and markedly changed the structure of microbial community. 16S rRNA gene clone library construction and phylogenetic analysis of soil bacteria revealed - Proteobacteria sequences dominated the cotton straw amendment soil, comprising 27.8% of the total number of analyzed sequences, while they were less represented in control soil (13.4%). On the contrary, the Sphingobacteria (7.8%) and Verrucomicrobia (2.4%) in the cotton straw amendment soil decreased after application when compared to the control soil 15.2% and 15.2%.

关键词： cotton straw     soil amendments     microbial diversity     Biolog     phospholipid fatty acid     16S rRNA gene clone library    

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Discrete element method modeling of corn-shaped particle flow in rectangular hopper

He TAO, Baosheng JIN, Wenqi ZHONG, Xiaofang WANG,

《结构与土木工程前沿（英文）》 2010年 第4卷 第2期   页码 267-275 doi: 10.1007/s11709-010-0035-0

摘要： Discrete element method (DEM) was developed to simulate the corn-shaped particles flow in the hopper. The corn-shaped particle was described by four overlapping spheres. Contact force and gravity force were considered when establishing the model. In addition, flowing characteristic of particles in the hopper was studied. The effect of friction coefficient on the wall pressure, voidage and velocity distribution was analyzed. The results show that the discharge rate decreases with the friction coefficient increasing; and the “over-pressure” phenomenon occurs in the discharging process for two different friction coefficients. The voidage also increases as the friction coefficient increasing. And the velocity distribution is more uniformity and is closer to the mass flow with the friction coefficient deceasing.

关键词： discrete         element          method         (DEM)             non-spherical     voidage     pressure     velocity distribution     hopper    

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标题 作者 时间 类型 操作

Performance and mechanism for cadmium and lead adsorption from water and soil by corn straw biochar

Tong Chi,Jiane Zuo,Fenglin Liu

期刊论文

METAGENOMICS COMBINED WITH HIGH-THROUGHPUT SEQUENCING REVEALS THE METHANOGENIC POTENTIAL OF FRESH CORNSTRAW UNDER THERMOPHILIC AND HIGH OLR

期刊论文

Removing phosphorus from aqueous solutions by using iron-modified corn straw biochar

Fenglin LIU,Jiane ZUO,Tong CHI,Pei WANG,Bo YANG

期刊论文

Experimental study on influence of operating parameters on tar components from corn straw gasification

Shuai GUO, Xiao WEI, Deyong CHE, Hongpeng LIU, Baizhong SUN

期刊论文

Kinetic studies of xylan hydrolysis of corn stover in a dilute acid cycle spray flow-through reactor

Hongman ZHANG, Qiang JIN, Rui XU, Lishi YAN, Zengxiang LIN

期刊论文

A neural network-based production process modeling and variable importance analysis approach in corn

期刊论文

Direct ethanol production from rice straw by coculture with two high-performing fungi

Maki TAKANO, Kazuhiro HOSHINO

期刊论文

Fabrication of cellulose aerogel from wheat straw with strong absorptive capacity

Jian LI,Caichao WAN,Yun LU,Qingfeng SUN

期刊论文

Isolation of highly purity cellulose from wheat straw using a modified aqueous biphasic system

Lifeng YAN, Yi ZHAO, Qing GU, Wan LI

期刊论文

Integrated benefits of power generation by straw biomass —A case study on the Sheyang Straw Power Plants

Xiaoshun LI , Futian QU , Dongmei JIANG , Peixin ZHU ,

期刊论文

Detoxification and concentration of corn stover hydrolysate and its fermentation for ethanol production

Qing Li, Yingjie Qin, Yunfei Liu, Jianjun Liu, Qing Liu, Pingli Li, Liqiang Liu

期刊论文

Biological pretreatment of corn stover by solid state fermentation of

Jian ZHANG, Xin REN, Wenqun CHEN, Jie BAO

期刊论文

Effect of mulching with maize straw on water infiltration and soil loss at different initial soil moistures

Yifu ZHANG,Hongwen LI,Jin HE,Qingjie WANG,Ying CHEN,Wanzhi CHEN,Shaochun MA

期刊论文

Effects of cotton straw amendment on soil fertility and microbial communities

Wuren HUANG, Zhihui BAI, Daniel HOEFEL, Qing HU, Xin LV, Guoqiang ZHUANG, Shengjun XU, Hongyan QI, Hongxun ZHANG

期刊论文

Discrete element method modeling of corn-shaped particle flow in rectangular hopper

He TAO, Baosheng JIN, Wenqi ZHONG, Xiaofang WANG,

期刊论文